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Soft Hydrothermal Synthesis of Hafnon, HfSiO4

Estevenon, Paul; Kaczmarek, Thibault; Rafiuddin, Mohamed Ruwaid; Welcomme, Eléonore; Szenknect, Stéphanie; Mesbah, Adel; Moisy, Philippe; Poinssot, Christophe; Dacheux, Nicolas


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        "name": "Rafiuddin, Mohamed Ruwaid", 
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        "name": "Welcomme, El\u00e9onore", 
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        "name": "Szenknect, St\u00e9phanie", 
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        "orcid": "0000-0003-3691-3621"
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        "name": "Mesbah, Adel", 
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        "name": "Moisy, Philippe", 
        "affiliation": "CEA, DEN, DMRC, Univ Montpellier, Marcoule 30207, France", 
        "orcid": "0000-0002-9331-0846"
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        "name": "Poinssot, Christophe", 
        "affiliation": "CEA, DEN, DMRC, Univ Montpellier, Marcoule 30207, France", 
        "orcid": "0000-0002-6161-9582"
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        "name": "Dacheux, Nicolas", 
        "affiliation": "ICSM Univ Montpellier, CNRS, CEA, ENSCM, Marcoule 30207, France", 
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    "publication_date": "2020-01-29", 
    "description": "<p>The conditions allowing the preparation of single phase HfSiO<sub>4</sub> has been determined through a multiparametric study by varying the concentrations of the reactants, the pH of the reactive media or the temperature and duration of the hydrothermal treatment. HfSiO<sub>4</sub> was prepared through relatively soft conditions (pH&nbsp;&le;&nbsp;1.6, C<sub>Si</sub>&nbsp;&asymp;&nbsp;C<sub>Hf</sub> &ge;<sup>&nbsp;</sup>0.21&nbsp;mol&middot;L<sup>\u20111</sup>, T &ge; 150&deg;C for t &ge; 24 hours).</p>"
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